Selective Pressurized Liquid Extraction as a Sample-Preparation Technique for Persistent Organic Pollutants and Contaminants of Emerging Concern

Document Type

Article

Journal/Book Title

Trends in Analytical Chemistry

Publication Date

5-1-2015

Publisher

Elsevier

Volume

68

First Page

119

Last Page

132

Abstract

Sample preparation represents about two-thirds of the cost of analysis and often presents logistical bottlenecks in analytical and environmental chemistry laboratories, thus reducing our capacity and preparedness to quantify organic pollutants rapidly and accurately. Selective pressurized liquid extraction (SPLE) is an analytical technique that builds upon PLE by incorporating matrix-compound (i.e. interference) retainers into the extraction step, thereby reducing sample-preparation steps and increasing sample throughput. SPLE methods offer distinct advantages over traditional methods, namely reduction in the costs intrinsic to sample preparation (i.e. time, solvents, labor, laboratory space, training, and potential loss of analytes). The ability to analyze and to evaluate rapidly a large number of samples directly increases the analytical capacity and preparedness of a laboratory for certain situations (e.g. large-scale studies or environmental emergencies). We review the analytical improvements via SPLE and its wide-ranging applications.

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